Information card for entry 7715255

Structure parameters

• Formula: C206 H209 K0.2 N7 O48 V8
• Calculated formula: C198 H197 K0.198 N3 O48 V8
• Title of publication: Reaction of Ph₂C(X)(CO₂H) (X = OH, NH₂) with [VO(OR)₃] (R = Et, <i>n</i>Pr): structure, magnetic susceptibility and ROP capability.
• Authors of publication: Glenister, Mollie A.; Frese, Josef W. A.; Elsegood, Mark R. J.; Canaj, Angelos B.; Brechin, Euan K.; Redshaw, Carl
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 12
• Pages of publication: 5351 - 5355
• a: 21.378 ± 0.003 Å
• b: 19.274 ± 0.003 Å
• c: 25.446 ± 0.004 Å
• α: 90°
• β: 111.554 ± 0.002°
• γ: 90°
• Cell volume: 9752 ± 3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1187
• Residual factor for significantly intense reflections: 0.0791
• Weighted residual factors for significantly intense reflections: 0.2133
• Weighted residual factors for all reflections included in the refinement: 0.2534
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.6943 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No