Information card for entry 7715319

Structure parameters

• Formula: C50.5 H87 B F12 P4 Si6
• Calculated formula: C48 H81 B F12 P4 Si6
• Title of publication: Triple <i>para</i>-substitution reactions of B(C₆F₅)₃ and [(C₆F₅)₃PF]⁺ with P(SiMe₃)₃.
• Authors of publication: Thomson, Jordan; Michailovich, Sofia; Miao, Linkun; Farrell, Jeffrey M.; Murray, Jillian A.; Lough, Alan; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 13
• Pages of publication: 5775 - 5778
• a: 16.808 ± 0.002 Å
• b: 16.808 ± 0.002 Å
• c: 81.648 ± 0.014 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 19976 ± 5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0326
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0801
• Weighted residual factors for all reflections included in the refinement: 0.0812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No