Information card for entry 7715331

Structure parameters

• Formula: C187.75 H171.75 F24 La2 N43.25 O27 S8 Zn
• Calculated formula: C187.75 H171.75 F24 La2 N43.25 O27 S8 Zn
• Title of publication: Programming heterometallic 4f-4f' helicates under thermodynamic control: the circle is complete.
• Authors of publication: Egger, Charlotte; Guénée, Laure; Deorukhkar, Neel; Piguet, Claude
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 13
• Pages of publication: 6050 - 6062
• a: 27.68761 ± 0.00013 Å
• b: 50.6972 ± 0.0003 Å
• c: 30.80194 ± 0.00017 Å
• α: 90°
• β: 104.644 ± 0.0005°
• γ: 90°
• Cell volume: 41831.7 ± 0.4 ų
• Cell temperature: 99.99 ± 0.1 K
• Ambient diffraction temperature: 99.99 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0722
• Residual factor for significantly intense reflections: 0.0669
• Weighted residual factors for significantly intense reflections: 0.1996
• Weighted residual factors for all reflections included in the refinement: 0.2058
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No