Information card for entry 7715791

Structure parameters

• Formula: C31 H35 Cl13 N4 Pd4 S4
• Calculated formula: C31 H35 Cl13 N4 Pd4 S4
• Title of publication: Reactivity of Schiff base-[C,N,S] pincer palladacycles: hydrolysis renders singular trinuclear, tetranuclear, and heteropentanuclear Pd3W2 coordinated complexes
• Authors of publication: Vila, Jose M.; Reigosa, Francisco; Pereira, M. Teresa; Polo, Paula M.
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 10.6947 ± 0.0008 Å
• b: 22.085 ± 0.0016 Å
• c: 40.285 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9515 ± 1.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0832
• Residual factor for significantly intense reflections: 0.0727
• Weighted residual factors for significantly intense reflections: 0.1326
• Weighted residual factors for all reflections included in the refinement: 0.1378
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0448
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No