Crystallography Open Database

Information card for entry 7715987

Preview

Coordinates	7715987.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	tBu4C4P6
Formula	C20 H36 P6
Calculated formula	C20 H36 P6
Title of publication	Access to 1,2,3-triphospholide ligands by reduction of di-tert-butyldiphosphatetrahedrane
Authors of publication	Uttendorfer, Maria Katharina; Hierlmeier, Gabriele; Balazs, Gabor; Wolf, Robert
Journal of publication	Dalton Transactions
Year of publication	2024
a	19.2177 ± 0.0005 Å
b	12.5176 ± 0.0003 Å
c	22.1442 ± 0.0006 Å
α	90°
β	112.755 ± 0.003°
γ	90°
Cell volume	4912.4 ± 0.2 Å³
Cell temperature	123 ± 0.1 K
Ambient diffraction temperature	123 ± 0.1 K
Number of distinct elements	3
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0471
Residual factor for significantly intense reflections	0.0411
Weighted residual factors for significantly intense reflections	0.1128
Weighted residual factors for all reflections included in the refinement	0.1174
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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