Information card for entry 7716219

Structure parameters

• Formula: C58 H89 N4 O1.5 S2 Si5
• Calculated formula: C58 H89 N4 O1.5 S2 Si5
• Title of publication: A Bis(silylene)silole - synthesis, properties and reactivity.
• Authors of publication: Liu, Chenghuan; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 25
• Pages of publication: 10446 - 10452
• a: 13.6292 ± 0.0007 Å
• b: 15.0182 ± 0.0008 Å
• c: 15.9881 ± 0.0008 Å
• α: 82.885 ± 0.002°
• β: 80.451 ± 0.002°
• γ: 75.486 ± 0.002°
• Cell volume: 3112.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0674
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.1314
• Weighted residual factors for all reflections included in the refinement: 0.1383
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No