Crystallography Open Database

Information card for entry 7716231

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Coordinates	7716231.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C84 H148 Br4 N4 Ni4 O8 P4
Calculated formula	C84 H148 Br4 N4 Ni4 O8 P4
Title of publication	Reactions of cyclonickelated complexes with hydroxyl amines and TEMPO• : isolation of new TEMPOH adducts of Ni(II) and their reactivities with nucleophiles and oxidants
Authors of publication	Sarker, Rajib Kumar; Zargarian, Davit
Journal of publication	Dalton Transactions
Year of publication	2024
a	15.1559 ± 0.0003 Å
b	11.6422 ± 0.0003 Å
c	15.0239 ± 0.0003 Å
α	90°
β	117.486 ± 0.001°
γ	90°
Cell volume	2351.71 ± 0.09 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0278
Residual factor for significantly intense reflections	0.0266
Weighted residual factors for significantly intense reflections	0.0705
Weighted residual factors for all reflections included in the refinement	0.0712
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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