Information card for entry 7716238

Structure parameters

• Formula: C23 H37 F3 N Ni O4 P
• Calculated formula: C23 H37 F3 N Ni O4 P
• Title of publication: Reactions of cyclonickelated complexes with hydroxyl amines and TEMPO• : isolation of new TEMPOH adducts of Ni(II) and their reactivities with nucleophiles and oxidants
• Authors of publication: Sarker, Rajib Kumar; Zargarian, Davit
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 15.7583 ± 0.0005 Å
• b: 12.7241 ± 0.0004 Å
• c: 14.183 ± 0.0005 Å
• α: 90°
• β: 115.546 ± 0.002°
• γ: 90°
• Cell volume: 2565.82 ± 0.15 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0942
• Residual factor for significantly intense reflections: 0.0568
• Weighted residual factors for significantly intense reflections: 0.1171
• Weighted residual factors for all reflections included in the refinement: 0.1291
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No