Information card for entry 7716310

Structure parameters

• Formula: C62 H42 B2 F30 N3 O Sb
• Calculated formula: C62 H42 B2 F30 N3 O Sb
• Title of publication: C–H Bond Activation at Antimony(III): Synthesis and Reactivity of Sb(III)-Oxyaryl Species
• Authors of publication: Dunes, Gabriel; Cordier, Marie; Kahlal, Samia; Pollnitz, Alpar; Saillard, Jean-Yves; Silvestru, Cristian; Sarazin, Yann
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 11.7279 ± 0.0012 Å
• b: 14.3207 ± 0.0015 Å
• c: 19.0667 ± 0.0019 Å
• α: 88.065 ± 0.004°
• β: 81.938 ± 0.004°
• γ: 78.543 ± 0.004°
• Cell volume: 3107.4 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0412
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0716
• Weighted residual factors for all reflections included in the refinement: 0.0743
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No