Information card for entry 7716312

Structure parameters

• Formula: C32 H44 N3 O S2 Sb
• Calculated formula: C32 H44 N3 O S2 Sb
• Title of publication: C–H Bond Activation at Antimony(III): Synthesis and Reactivity of Sb(III)-Oxyaryl Species
• Authors of publication: Dunes, Gabriel; Cordier, Marie; Kahlal, Samia; Pollnitz, Alpar; Saillard, Jean-Yves; Silvestru, Cristian; Sarazin, Yann
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 10.2127 ± 0.001 Å
• b: 25.78 ± 0.002 Å
• c: 12.4202 ± 0.0013 Å
• α: 90°
• β: 93.905 ± 0.004°
• γ: 90°
• Cell volume: 3262.4 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0275
• Residual factor for significantly intense reflections: 0.0238
• Weighted residual factors for significantly intense reflections: 0.0494
• Weighted residual factors for all reflections included in the refinement: 0.0507
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No