Information card for entry 7716314

Structure parameters

• Formula: C92 H128 N4 O4 Sb4
• Calculated formula: C92 H128 N4 O4 Sb4
• Title of publication: C–H Bond Activation at Antimony(III): Synthesis and Reactivity of Sb(III)-Oxyaryl Species
• Authors of publication: Dunes, Gabriel; Cordier, Marie; Kahlal, Samia; Pollnitz, Alpar; Saillard, Jean-Yves; Silvestru, Cristian; Sarazin, Yann
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 21.5783 ± 0.0013 Å
• b: 21.5783 Å
• c: 9.3024 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4331.4 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 82
• Hermann-Mauguin space group symbol: I -4
• Hall space group symbol: I -4
• Residual factor for all reflections: 0.0275
• Residual factor for significantly intense reflections: 0.0259
• Weighted residual factors for significantly intense reflections: 0.0647
• Weighted residual factors for all reflections included in the refinement: 0.0659
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No