Information card for entry 7716394

Structure parameters

• Formula: C34 H33 F12 N O2 Si
• Calculated formula: C34 H33 F12 N O2 Si
• Title of publication: Synthesis, structure, and alkynylation reactivity of alkynyl-silicate, -germanate, and -stannate.
• Authors of publication: Iwabuchi, Shuta; Morofuji, Tatsuya; Kano, Naokazu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• a: 11.0531 ± 0.0002 Å
• b: 16.2521 ± 0.0003 Å
• c: 18.3816 ± 0.0003 Å
• α: 90°
• β: 95.844 ± 0.002°
• γ: 90°
• Cell volume: 3284.84 ± 0.1 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0596
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.0983
• Weighted residual factors for all reflections included in the refinement: 0.0998
• Goodness-of-fit parameter for all reflections included in the refinement: 1.283
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No