Information card for entry 7716396

Structure parameters

• Formula: C34 H33 F12 Ge N O2
• Calculated formula: C34 H33 F12 Ge N O2
• Title of publication: Synthesis, structure, and alkynylation reactivity of alkynyl-silicate, -germanate, and -stannate.
• Authors of publication: Iwabuchi, Shuta; Morofuji, Tatsuya; Kano, Naokazu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• a: 11.1071 ± 0.0005 Å
• b: 16.2492 ± 0.0009 Å
• c: 18.3357 ± 0.0008 Å
• α: 90°
• β: 95.828 ± 0.004°
• γ: 90°
• Cell volume: 3292.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0673
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.0759
• Weighted residual factors for all reflections included in the refinement: 0.0819
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No