Information card for entry 7716447

Structure parameters

• Formula: C21 H23 B2 N14 Y
• Calculated formula: C21 H23 B2 N14 Y
• Title of publication: Activation and functionalisation of carbon dioxide by bis-tris(pyrazolyl)borate-supported divalent samarium and trivalent lanthanide silylamide complexes.
• Authors of publication: Chowdhury, Tajrian; Wilson, Claire; Farnaby, Joy H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 28
• Pages of publication: 11884 - 11894
• a: 13.007 ± 0.003 Å
• b: 9.3117 ± 0.0017 Å
• c: 21.482 ± 0.004 Å
• α: 90°
• β: 96.332 ± 0.007°
• γ: 90°
• Cell volume: 2586 ± 0.9 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1266
• Residual factor for significantly intense reflections: 0.0842
• Weighted residual factors for significantly intense reflections: 0.1868
• Weighted residual factors for all reflections included in the refinement: 0.2119
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No