Information card for entry 7716728

Structure parameters

• Formula: C29 H25 Cl O2 Ru
• Calculated formula: C29 H25 Cl O2 Ru
• Title of publication: Phenalenyl-ruthenium synergism for effectual catalytic transformations of primary amines to amides.
• Authors of publication: Bandopadhyay, Nilaj; Paramanik, Krishnendu; Sarkar, Gayetri; Roy, Suvojit; Panda, Subhra Jyoti; Purohit, Chandra Shekhar; Biswas, Bhaskar; Das, Hari Sankar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 33
• Pages of publication: 13795 - 13804
• a: 12.7749 ± 0.0004 Å
• b: 10.758 ± 0.0003 Å
• c: 16.9453 ± 0.0005 Å
• α: 90°
• β: 101.721 ± 0.003°
• γ: 90°
• Cell volume: 2280.27 ± 0.12 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0301
• Residual factor for significantly intense reflections: 0.0291
• Weighted residual factors for significantly intense reflections: 0.0771
• Weighted residual factors for all reflections included in the refinement: 0.0777
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No