Information card for entry 7716743

Structure parameters

• Formula: C84 H104 Cl8 F12 N8 Ni2 O4 Sb2
• Calculated formula: C81 H98 Cl2 F12 N8 Ni2 O4 Sb2
• Title of publication: Ni(II) and Pd(II) complexes of a new redox-active pentadentate azo-appended 2-aminophenol ligand: Pd(II)-assisted intraligand cyclization forms a phenoxazinyl ring.
• Authors of publication: Bhowmik, Saumitra; Sengupta, Arunava; Mukherjee, Rabindranath
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 33
• Pages of publication: 14046 - 14064
• a: 9.5233 ± 0.0014 Å
• b: 18.212 ± 0.003 Å
• c: 27.463 ± 0.004 Å
• α: 81.734 ± 0.004°
• β: 83.363 ± 0.004°
• γ: 85.055 ± 0.004°
• Cell volume: 4670.3 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0513
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.0903
• Weighted residual factors for all reflections included in the refinement: 0.0983
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No