Information card for entry 7716792

Structure parameters

• Formula: C14 H22 O6 Pd
• Calculated formula: C14 H22 O6 Pd
• Title of publication: New palladium(II) β-ketoesterates for focused electron beam induced deposition: synthesis, structures, and characterization.
• Authors of publication: Butrymowicz-Kubiak, A; Muzioł, T M; Kaczmarek-Kędziera, A; Jureddy, C. S.; Maćkosz, K; Utke, I.; Szymańska, I B
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 32
• Pages of publication: 13662 - 13677
• a: 4.35329 ± 0.0001 Å
• b: 10.3794 ± 0.0003 Å
• c: 17.7657 ± 0.0005 Å
• α: 90°
• β: 93.392 ± 0.002°
• γ: 90°
• Cell volume: 801.33 ± 0.04 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0384
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0948
• Weighted residual factors for all reflections included in the refinement: 0.0981
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No