Information card for entry 7716903

Structure parameters

• Formula: C20 H24 Cl N2 Ni O6 P S2
• Calculated formula: C20 H24 Cl N2 Ni O6 P S2
• Title of publication: Synthesis and reactivity of air stable Ni(II) complexes with isocyanides and dialkyldithiophosphate ligands: acyclic diaminocarbene formation
• Authors of publication: Alvarez-Miguel, Lucia; del Carmen-Rodríguez, Clara; Valle, Maria; Alvarez, Celedonio M.; Martín Álvarez, Jose Miguel; García-Rodríguez, Raúl; Miguel, Daniel
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 7.2158 ± 0.0003 Å
• b: 10.0031 ± 0.0008 Å
• c: 18.9825 ± 0.001 Å
• α: 99.859 ± 0.005°
• β: 97.908 ± 0.004°
• γ: 105.106 ± 0.005°
• Cell volume: 1279.15 ± 0.14 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0919
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.1531
• Weighted residual factors for all reflections included in the refinement: 0.1815
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No