Nickel(II) complexes with 14-membered bis-thiosemicarbazide and bis-isothiosemicarbazide ligands: synthesis, characterization and catalysis of oxygen evolution reaction.
Authors of publication
Besleaga, Iuliana; Fesenko, Anastasia A.; Paul, Anup; Šljukić, Biljana; Rapta, Peter; Pombeiro, Armando J. L.; Shutalev, Anatoly D.; Arion, Vladimir B.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2024
a
17.0619 ± 0.0009 Å
b
9.7583 ± 0.0003 Å
c
21.8947 ± 0.0007 Å
α
90°
β
90°
γ
90°
Cell volume
3645.4 ± 0.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
61
Hermann-Mauguin space group symbol
P b c a
Hall space group symbol
-P 2ac 2ab
Residual factor for all reflections
0.032
Residual factor for significantly intense reflections
0.0282
Weighted residual factors for significantly intense reflections
0.0739
Weighted residual factors for all reflections included in the refinement
0.0758
Goodness-of-fit parameter for all reflections included in the refinement
