Crystallography Open Database

Information card for entry 7717005

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Coordinates	7717005.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H68 Cl3 Fe N4 P2 Si2
Calculated formula	C38 H68 Cl3 Fe N4 P2 Si2
Title of publication	Dinitrogen silylation catalyzed by silylene cobalt(I) and silylene iron(I) chlorides
Authors of publication	Fan, Qingqing; Li, Qingshuang; Sun, Hongjian; Li, Xiaoyan
Journal of publication	Dalton Transactions
Year of publication	2024
a	13.6644 ± 0.0002 Å
b	20.274 ± 0.0003 Å
c	16.7641 ± 0.0002 Å
α	90°
β	92.553 ± 0.001°
γ	90°
Cell volume	4639.58 ± 0.11 Å³
Cell temperature	173 ± 0.1 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0577
Residual factor for significantly intense reflections	0.0499
Weighted residual factors for significantly intense reflections	0.1381
Weighted residual factors for all reflections included in the refinement	0.1439
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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