Information card for entry 7717011

Structure parameters

• Formula: C12 H19 Cl F10 O P Sb
• Calculated formula: C12 H19 Cl F10 O P Sb
• Title of publication: Adducts of Lewis acidic stibanes with phosphane chalcogenides
• Authors of publication: Krieft, Jonas; Koch, Hannah; Neumann, Beate; Stammler, Georg; Lamm, Jan-Hendrik; Mix, Andreas; Mitzel, Norbert Werner
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 7.7947 ± 0.0003 Å
• b: 17.4038 ± 0.0007 Å
• c: 15.4407 ± 0.0006 Å
• α: 90°
• β: 97.791 ± 0.004°
• γ: 90°
• Cell volume: 2075.31 ± 0.14 ų
• Cell temperature: 173 ± 0.1 K
• Ambient diffraction temperature: 173 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0488
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0711
• Weighted residual factors for all reflections included in the refinement: 0.0809
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No