Information card for entry 7717013

Structure parameters

• Formula: C24 H25 Cl F12 P S Sb
• Calculated formula: C24 H25 Cl F12 P S Sb
• Title of publication: Adducts of Lewis acidic stibanes with phosphane chalcogenides.
• Authors of publication: Krieft, Jonas; Koch, Hannah; Neumann, Beate; Stammler, Hans-Georg; Lamm, Jan-Hendrik; Mix, Andreas; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 39
• Pages of publication: 16280 - 16286
• a: 12.351 ± 0.004 Å
• b: 20.7885 ± 0.0015 Å
• c: 13.006 ± 0.003 Å
• α: 90°
• β: 113.5 ± 0.03°
• γ: 90°
• Cell volume: 3062.4 ± 1.4 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0833
• Weighted residual factors for all reflections included in the refinement: 0.0893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.132
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No