Information card for entry 7717065

Structure parameters

• Formula: C12 H36 Co Mo6 O25 S6
• Calculated formula: C12 H36 Co Mo6 O25 S6
• Title of publication: Polyoxometalate-supported transition metal complexes for the oxidative cross-coupling of amines and alcohols.
• Authors of publication: Pardiwala, Ankita; Desai, Meghal A.; Jangir, Ritambhara
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 42
• Pages of publication: 17207 - 17220
• a: 8.6329 ± 0.0009 Å
• b: 9.2575 ± 0.0009 Å
• c: 12.2531 ± 0.0013 Å
• α: 94.763 ± 0.004°
• β: 93.152 ± 0.004°
• γ: 91.312 ± 0.004°
• Cell volume: 974.03 ± 0.17 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0578
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.138
• Weighted residual factors for all reflections included in the refinement: 0.1404
• Goodness-of-fit parameter for all reflections included in the refinement: 1.236
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No