Information card for entry 7717216

Structure parameters

• Formula: C48 H214 Cu8 K2 N32 Nb24 O109 P2 V4
• Calculated formula: C48 H136 Cu8 K2 N32 Nb24 O109 P2 V4
• Title of publication: Three organic-inorganic polyoxoniobate-based compounds modified with Cu(II) amine complexes: synthesis, characterization, and catalytic studies for oxidation of styrene.
• Authors of publication: Duan, Zhi-Cheng; Li, Guanghua; Li, Ke-Chang; Cui, Xiao-Bing
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 44
• Pages of publication: 17880 - 17892
• a: 26.3917 ± 0.0006 Å
• b: 26.3917 ± 0.0006 Å
• c: 27.4474 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 19117.7 ± 1 ų
• Cell temperature: 299 K
• Ambient diffraction temperature: 299 K
• Number of distinct elements: 9
• Space group number: 140
• Hermann-Mauguin space group symbol: I 4/m c m
• Hall space group symbol: -I 4 2c
• Residual factor for all reflections: 0.0821
• Residual factor for significantly intense reflections: 0.0642
• Weighted residual factors for significantly intense reflections: 0.1778
• Weighted residual factors for all reflections included in the refinement: 0.2061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.114
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No