Information card for entry 7717243

Structure parameters

• Formula: C42 H38 Cl5 N Ni O P2
• Calculated formula: C42 H38 Cl5 N Ni O P2
• Title of publication: NiII, PdII and PtII pincer complexes of 2-(diphenylphosphaneyl)-N-(2-(diphenyl-phosphaneyl)benzyl)benzamide: synthesis, reactivity and catalytic studies
• Authors of publication: Dwivedi, Khilesh Chandra; Sabharwal, Gazal; Kote, Basvaraj S.; Balakrishna, Maravanji Shivaramaiah
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 12.6703 ± 0.0004 Å
• b: 12.9622 ± 0.0004 Å
• c: 13.9961 ± 0.0003 Å
• α: 76.582 ± 0.002°
• β: 77.268 ± 0.002°
• γ: 62.127 ± 0.003°
• Cell volume: 1959.7 ± 0.11 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0539
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.1034
• Weighted residual factors for all reflections included in the refinement: 0.1129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No