Information card for entry 7717247

Structure parameters

• Formula: C40 H34 Cl5 N O P2 Pd
• Calculated formula: C39 H32 Cl3 N O P2 Pd
• Title of publication: NiII, PdII and PtII pincer complexes of 2-(diphenylphosphaneyl)-N-(2-(diphenyl-phosphaneyl)benzyl)benzamide: synthesis, reactivity and catalytic studies
• Authors of publication: Dwivedi, Khilesh Chandra; Sabharwal, Gazal; Kote, Basvaraj S.; Balakrishna, Maravanji Shivaramaiah
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 12.6618 ± 0.0007 Å
• b: 12.8044 ± 0.0007 Å
• c: 13.8971 ± 0.0007 Å
• α: 77.55 ± 0.002°
• β: 76.927 ± 0.002°
• γ: 60.683 ± 0.002°
• Cell volume: 1898.98 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0339
• Residual factor for significantly intense reflections: 0.0283
• Weighted residual factors for significantly intense reflections: 0.0702
• Weighted residual factors for all reflections included in the refinement: 0.0728
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No