Information card for entry 7717254

Structure parameters

• Formula: C12 H48 N3 O40 V7
• Calculated formula: C12 H48 N3 O40 V7
• Title of publication: Iso- and hetero-polyoxovanadium glycolates [VIV6O₆(glyc)₆M^III(OH)₆]^3- (M = V, Cr, Fe, and Al) encapsulating metal hydroxides.
• Authors of publication: Jin, Wan-Ting; Xie, Zhen-Lang; Su, Xing; Gao, Chuan-Hua; Hu, Jing; Zhou, Zhao-Hui
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 46
• Pages of publication: 18711 - 18719
• a: 21.2465 ± 0.0018 Å
• b: 9.7088 ± 0.0005 Å
• c: 22.0761 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4553.8 ± 0.5 ų
• Cell temperature: 223 K
• Ambient diffraction temperature: 223 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1067
• Residual factor for significantly intense reflections: 0.0961
• Weighted residual factors for significantly intense reflections: 0.2678
• Weighted residual factors for all reflections included in the refinement: 0.2907
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No