Crystallography Open Database

Information card for entry 7717334

Preview

Coordinates	7717334.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H80 K2 O10 P2
Calculated formula	C52 H80 K2 O10 P2
Title of publication	Syntheses and Structures of Dimesitylphosphinite Complexes of the Alkali Metals as well as Their Catalytic Activity in Hydro-phosphorylation Reactions
Authors of publication	Fener, Benjamin; Schüler, Philipp; Liebing, Phil; Görls, Helmar; Westerhausen, Matthias
Journal of publication	Dalton Transactions
Year of publication	2024
a	11.8451 ± 0.0002 Å
b	19.0701 ± 0.0003 Å
c	24.4414 ± 0.0003 Å
α	90°
β	97.814 ± 0.001°
γ	90°
Cell volume	5469.74 ± 0.14 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	5
Space group number	7
Hermann-Mauguin space group symbol	P 1 n 1
Hall space group symbol	P -2yac
Residual factor for all reflections	0.0945
Residual factor for significantly intense reflections	0.0702
Weighted residual factors for significantly intense reflections	0.1324
Weighted residual factors for all reflections included in the refinement	0.1461
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7717334.html