Information card for entry 7717336

Structure parameters

• Formula: C172 H234 K8 O16 P8
• Calculated formula: C172 H234 K8 O16 P8
• Title of publication: Syntheses and Structures of Dimesitylphosphinite Complexes of the Alkali Metals as well as Their Catalytic Activity in Hydro-phosphorylation Reactions
• Authors of publication: Fener, Benjamin; Schüler, Philipp; Liebing, Phil; Görls, Helmar; Westerhausen, Matthias
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 16.0585 ± 0.0002 Å
• b: 20.2473 ± 0.0003 Å
• c: 28.3626 ± 0.0003 Å
• α: 90°
• β: 104.325 ± 0.001°
• γ: 90°
• Cell volume: 8935.1 ± 0.2 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1179
• Residual factor for significantly intense reflections: 0.0727
• Weighted residual factors for significantly intense reflections: 0.1498
• Weighted residual factors for all reflections included in the refinement: 0.1688
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No