Information card for entry 7717344

Structure parameters

• Formula: C60 H92 O2 P2 Rb2
• Calculated formula: C60 H92 O2 P2 Rb2
• Title of publication: Syntheses and Structures of Dimesitylphosphinite Complexes of the Alkali Metals as well as Their Catalytic Activity in Hydro-phosphorylation Reactions
• Authors of publication: Fener, Benjamin; Schüler, Philipp; Liebing, Phil; Görls, Helmar; Westerhausen, Matthias
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 13.7831 ± 0.0013 Å
• b: 14.0866 ± 0.0014 Å
• c: 18.4745 ± 0.0017 Å
• α: 80.831 ± 0.004°
• β: 83.722 ± 0.004°
• γ: 83.847 ± 0.005°
• Cell volume: 3505.1 ± 0.6 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.116
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1658
• Weighted residual factors for all reflections included in the refinement: 0.1888
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No