Information card for entry 7717499

Structure parameters

• Formula: C25 H38 Cl3 N3 O3 P2 Pd
• Calculated formula: C25 H38 Cl3 N3 O3 P2 Pd
• Title of publication: Simple and easy functionalization of para–hydroxy POCOP–M (M=Ni(II), Pd(II)) pincer complexes: Synthesis of multimetallic species
• Authors of publication: Serrano-García, Juan Sebastián; Garcia Eleno , Marco Antonio; Arenaza-Corona, Antonino; Rufino-Felipe, Ernesto; Valdes, Hugo; Hernandez Ortega, Simon; Morales-Morales, David
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 8.1646 ± 0.001 Å
• b: 28.713 ± 0.004 Å
• c: 13.7242 ± 0.0017 Å
• α: 90°
• β: 95.542 ± 0.002°
• γ: 90°
• Cell volume: 3202.3 ± 0.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1333
• Residual factor for significantly intense reflections: 0.0698
• Weighted residual factors for significantly intense reflections: 0.158
• Weighted residual factors for all reflections included in the refinement: 0.1926
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No