Information card for entry 7717534

Structure parameters

• Formula: C24 H72 Ge2 N4 S2 Si8
• Calculated formula: C24 H72 Ge2 N4 S2 Si8
• Title of publication: Desulfurization of Isothiocyanates by a Divalent Germanium Amide
• Authors of publication: Stacil, Thad; Fortney, Vanessa; Murphy, Julia; Gembicky, Milan; Rheingold, Arnold; Weinert, Charles
• Journal of publication: Dalton Transactions
• Year of publication: 2024
• a: 9.0563 ± 0.0016 Å
• b: 41.16 ± 0.007 Å
• c: 12.51 ± 0.002 Å
• α: 90°
• β: 106.559 ± 0.002°
• γ: 90°
• Cell volume: 4469.8 ± 1.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0257
• Weighted residual factors for significantly intense reflections: 0.0622
• Weighted residual factors for all reflections included in the refinement: 0.065
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No