Information card for entry 7717739

Structure parameters

• Formula: C32 H61 Ge K N2 O6 Si3
• Calculated formula: C32 H61 Ge K N2 O6 Si3
• Title of publication: Synthesis and exploration of a 1<i>H</i>-germol-1-ide/pyridine bidentate ligand.
• Authors of publication: Liu, Chenghuan; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 5
• Pages of publication: 2005 - 2010
• a: 19.6032 ± 0.0009 Å
• b: 10.9806 ± 0.0005 Å
• c: 20.4878 ± 0.0008 Å
• α: 90°
• β: 110.145 ± 0.0014°
• γ: 90°
• Cell volume: 4140.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0546
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.0817
• Weighted residual factors for all reflections included in the refinement: 0.0867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No