Information card for entry 8101102

Structure parameters

• Formula: C52 H82 Li O1.5 Si2 Ti2
• Calculated formula: C52 H82 Li O1.5 Si2 Ti2
• Title of publication: Crystal structure of [2,2-bis(η^5^-pentamethylcyclopentadienyl)- bis-(μ,η^1^:η^2^-2-trimethylsilyl-ethinyl)titanium(IV) lithium] [2,2-bis(η^5^-pentamethylcyclopentadienyl)-oxotitanium(III)— tetrahydrofurane (1/0.5), C~50~H~78~LiOSi~2~Ti~2~ · 0.5C~4~H~8~O
• Authors of publication: Spannenberg, Anke; Burlakov, Vladimir V.; Rosenthal, Uwe
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2001
• Journal volume: 216
• Journal issue: 4
• Pages of publication: 616 - 618
• a: 10.314 ± 0.002 Å
• b: 23.451 ± 0.005 Å
• c: 23.651 ± 0.005 Å
• α: 90°
• β: 100.36 ± 0.03°
• γ: 90°
• Cell volume: 5627.3 ± 2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for significantly intense reflections: 0.1601
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No