Information card for entry 8101188

Structure parameters

• Formula: C33 H48 F2 N2 O2.5 Si
• Calculated formula: C33 H48 F2 N2 O2.5 Si
• Title of publication: Crystal structure of N,N'-ethylenebis(3,5-di-tert-butylsalicylideneiminato) difluorosilane—dioxane (4/1), 4C~32~H~46~F~2~N~2~O~2~Si~4~ · C~4~H~8~O~2~
• Authors of publication: Haberecht, Jörg; Böhme, Uwe; Lang, Heinrich; Rheinwald, Gerd; Roewer, Gerhard
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2000
• Journal volume: 215
• Journal issue: 1
• Pages of publication: 135 - 137
• a: 14.1657 ± 0.0002 Å
• b: 16.1074 ± 0.0002 Å
• c: 17.1227 ± 0.0001 Å
• α: 89.4677 ± 0.0005°
• β: 65.9674 ± 0.0005°
• γ: 79.0775 ± 0.0002°
• Cell volume: 3493.56 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0577
• Weighted residual factors for significantly intense reflections: 0.1278
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No