Information card for entry 8101479

Structure parameters

• Formula: C32 H70 N6 Na Nb O2
• Calculated formula: C32 H70 N6 Na Nb O2
• SMILES: C1N(C(C)C)[Nb]23(N(C(C)C)CCN3C(C)C)(N(C(C)C)CC[N]32C(C)C)[N](C(C)C)(C1)[Na]3([O]1CCCC1)[O]1CCCC1
• Title of publication: Crystal structure of N,N'-diisopropylethylenediamido-μ(1kN',2kN)-bis(N,N'- diisopropylethenediamido-1kN,2kN')niobium(V)-bis(tetrahydrofuran)sodium(I), [Nb(iPr2en)3{Na(thf)2}]
• Authors of publication: Armstrong, William H.; Bonitatebus, Peter J. Jr.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 1999
• Journal volume: 214
• Journal issue: 2
• Pages of publication: 243 - 244
• a: 16.38 ± 0.003 Å
• b: 13.003 ± 0.004 Å
• c: 18.23 ± 0.004 Å
• α: 90°
• β: 104.23 ± 0.015°
• γ: 90°
• Cell volume: 3763.7 ± 1.4 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for significantly intense reflections: 0.1124
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No