Information card for entry 8101665

Structure parameters

• Formula: C39.5 H45 P S Si2
• Calculated formula: C39.5 H45 P S Si2
• Title of publication: Crystal structure of tetraphenylphosphonium-2,6-bis(trimethylsilyl) thiophenolate-toluene (1/0.5), [Ph~4~P][SC~6~H~3~(SiMe~3~)~2~] · 0.5C~7~H~8~
• Authors of publication: Hauptmann, Ralf; Schneider, Jörg; Köckerling, Martin; Henkel, Gerald
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 1998
• Journal volume: 213
• Journal issue: 4
• Pages of publication: 781 - 782
• a: 11.833 ± 0.001 Å
• b: 13.699 ± 0.002 Å
• c: 22.631 ± 0.003 Å
• α: 90°
• β: 91.18 ± 0.01°
• γ: 90°
• Cell volume: 3667.7 ± 0.6 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for significantly intense reflections: 0.0892
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No