Information card for entry 8101837

Structure parameters

• Chemical name: poly[[aqua(1,10-phenanthroline-κ^2^N,N')nickel(II)]- μ-(dihydrogen-benzene-1,2,4,5-tetracarboxylato)-κ^3^O^1^:O^2^:O^3^]
• Formula: C22 H14 N2 Ni O9
• Calculated formula: C22 H14 N2 Ni O9
• Title of publication: Crystal structure of poly[{aqua(1,10-phenanthroline-k^2^N,N')nickel (II)}-μ-(dihydrogen-benzene-1,2,4,5-tetracarboxylate)-k^3^O:O':O''], Ni(C10H4O8)(C12H8N2)(H2O)
• Authors of publication: J.-C. Lee; H. Takahashi; Y. Matsui
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2005
• Journal volume: 220
• Journal issue: 3
• Pages of publication: 489 - 490
• a: 9.589 ± 0.005 Å
• b: 10.144 ± 0.007 Å
• c: 11.312 ± 0.005 Å
• α: 87.11 ± 0.02°
• β: 72.38 ± 0.02°
• γ: 64.96 ± 0.02°
• Cell volume: 946.3 ± 0.9 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0367
• Residual factor for significantly intense reflections: 0.0347
• Weighted residual factors for all reflections: 0.0863
• Weighted residual factors for significantly intense reflections: 0.0854
• Weighted residual factors for all reflections included in the refinement: 0.0854
• Goodness-of-fit parameter for all reflections included in the refinement: 0.8459
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No