Information card for entry 8101896

Structure parameters

• Chemical name: methanol[4-bromo-N-(2-pyridylmethyl)salicylaldiminato-N,N',O]nickel(II) monoperchlorate
• Formula: C14 H14 Br Cl N2 Ni O6
• Calculated formula: C14 H14 Br Cl N2 Ni O6
• Title of publication: Crystal structure of methanol[4-bromo-N-(2-pyridylmethyl)salicylaldiminato- N,N',O]nickel(II) perchlorate, [Ni(CH~3~OH)(C~14~H~14~BrN~2~O~2~)]ClO~4~
• Authors of publication: Peng, S.-J.; Yang, D.-W.; Xiao, Z.-L.; Wu, D.-X.; Cao, Z.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2005
• Journal volume: 220
• Journal issue: 4
• Pages of publication: 633 - 634
• a: 7.204 ± 0.001 Å
• b: 19.11 ± 0.002 Å
• c: 12.704 ± 0.002 Å
• α: 90°
• β: 95.897 ± 0.002°
• γ: 90°
• Cell volume: 1739.7 ± 0.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0691
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for significantly intense reflections: 0.0979
• Weighted residual factors for all reflections included in the refinement: 0.1093
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No