Information card for entry 8101991

Structure parameters

• Chemical name: hexakis(μ~2~-acetato)-tris(acetonitrile-κN)-μ~3~-oxo-trialuminum(III) tetrachloroaluminate
• Formula: C18 H27 Al4 Cl4 N3 O13
• Calculated formula: C18 H27 Al4 Cl3.96 N3 O13
• Title of publication: Crystal structure of hexakis(μ~2~-acetato)tris(acetonitrile- κN)-μ~3~-oxo-trialuminum(III) tetrachloroaluminate, [Al~3~(C~2~H~3~O~2~)~6~(C~2~H~3~N)~3~O][AlCl~4~]
• Authors of publication: Lemoine, P.; Bekaert, A.; Brion, J. D.; Viossat, B.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2006
• Journal volume: 221
• Journal issue: 3
• Pages of publication: 309 - 310
• a: 11.867 ± 0.005 Å
• b: 15.421 ± 0.005 Å
• c: 19.181 ± 0.005 Å
• α: 90 ± 0.005°
• β: 90 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 3510 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 20
• Hermann-Mauguin space group symbol: C 2 2 21
• Hall space group symbol: C 2c 2
• Residual factor for all reflections: 0.1157
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.1247
• Weighted residual factors for all reflections included in the refinement: 0.1404
• Goodness-of-fit parameter for all reflections included in the refinement: 0.959
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No