Information card for entry 8102093

Structure parameters

• Formula: C20 H22 N2 O6 Pb S2
• Calculated formula: C20 H22 N2 O6 Pb S2
• Title of publication: Crystal structure of catena-(μ-(N,N-dimethylformamide)-N,N- dimethylformamide-μ-(2,2'-dithiodibenzoato)-lead(II)), Pb[ (CH~3~)~2~NCHO]~2~[S~2~(C~6~H~4~COO)~2~]
• Authors of publication: Li, X.-H.; Jia, S.-C.; Jalbout, A. F.
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2007
• Journal volume: 222
• Journal issue: 2
• Pages of publication: 117 - 118
• a: 9.7413 ± 0.0004 Å
• b: 11.7 ± 0.0004 Å
• c: 12.4184 ± 0.0005 Å
• α: 65.207 ± 0.001°
• β: 70.108 ± 0.001°
• γ: 65.546 ± 0.002°
• Cell volume: 1145.61 ± 0.08 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0276
• Residual factor for significantly intense reflections: 0.0257
• Weighted residual factors for significantly intense reflections: 0.0647
• Weighted residual factors for all reflections included in the refinement: 0.0655
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No