Information card for entry 8102144

Structure parameters

• Chemical name: tetra-μ~3~-bromo-tetrakis(tert-butyl-(4-methyl-pyridin-2-yl)-amine)- tetracopper(I)
• Formula: C40 H64 Br4 Cu4 N8
• Calculated formula: C40 H64 Br4 Cu4 N8
• Title of publication: Crystal structure of tetra-μ~3~-bromo-tetrakis(tert-butyl- (4-methyl-pyridin-2-yl)-amine)-tetracopper(I), Cu~4~Br~4~(C~10~H~16~N~2~) ~4~
• Authors of publication: Glatz, Germund; Irrgang, Torsten; Kempe, Rhett
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2007
• Journal volume: 222
• Journal issue: 3
• Pages of publication: 261 - 262
• a: 15.325 ± 0.001 Å
• b: 15.325 ± 0.001 Å
• c: 10.505 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2467.2 ± 0.3 ų
• Cell temperature: 191 ± 2 K
• Ambient diffraction temperature: 191 ± 2 K
• Number of distinct elements: 5
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0762
• Residual factor for significantly intense reflections: 0.0556
• Weighted residual factors for significantly intense reflections: 0.1492
• Weighted residual factors for all reflections included in the refinement: 0.1615
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No