Information card for entry 8102223

Structure parameters

• Chemical name: tris(ethylenediamine)nickel(II) diperchlorate 2-(4-pyridyl)-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide solvate monohydrate
• Formula: C18 H42 Cl2 N9 Ni O11
• Calculated formula: C18 H42 Cl2 N9 Ni O11
• Title of publication: Crystal structure of tris(ethylenediamine)nickel(II) diperchlorate 2-(4-pyridyl)-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide solvate monohydrate, [Ni(C~2~H~8~N~2~)~3~][ClO~4~]~2~ · C~12~H~16~N~3~O~2~ · H~2~O
• Authors of publication: Wang, Yu-Fang; Liu, Yuan-Ying
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2007
• Journal volume: 222
• Journal issue: 4
• Pages of publication: 439 - 441
• a: 9.897 ± 0.002 Å
• b: 15.461 ± 0.004 Å
• c: 10.407 ± 0.002 Å
• α: 90°
• β: 99.292 ± 0.003°
• γ: 90°
• Cell volume: 1571.6 ± 0.6 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0933
• Residual factor for significantly intense reflections: 0.0728
• Weighted residual factors for significantly intense reflections: 0.1819
• Weighted residual factors for all reflections included in the refinement: 0.2037
• Goodness-of-fit parameter for all reflections included in the refinement: 0.995
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No