Information card for entry 8102267

Structure parameters

• Formula: C24 H24 Cl2 Cu N16 O8 S16
• Calculated formula: C24 H24 Cl2 Cu N16 O8 S16
• Title of publication: Crystal structure of 2,2'-(1,2-diethanediyl-bis(thio)-bis-(1,3,4-thiadiazole) copper(II) diperchlorate, [Cu(C6H6N4S4)4][ClO4]2
• Authors of publication: Jian-Ge Wang; Jian-Hua Qin; Pu-Zhou Hu; Bang-Tun Zhao
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2008
• Journal volume: 223
• Journal issue: 3
• Pages of publication: 225
• a: 10.4488 ± 0.0017 Å
• b: 10.4744 ± 0.0017 Å
• c: 12.705 ± 0.002 Å
• α: 68.694 ± 0.002°
• β: 76.439 ± 0.002°
• γ: 74.924 ± 0.002°
• Cell volume: 1235.6 ± 0.3 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0513
• Residual factor for significantly intense reflections: 0.0401
• Weighted residual factors for significantly intense reflections: 0.0985
• Weighted residual factors for all reflections included in the refinement: 0.1069
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No