Information card for entry 8102275

Structure parameters

• Common name: tris(1,10-phenanthroline-5,6-dione)-zinc(II) diperchlorate
• Formula: C36 H18 Cl2 N6 O14 Zn
• Calculated formula: C36 H18 Cl2 N6 O14 Zn
• Title of publication: Crystal structure of tris(1,10-phenanthroline-5,6-dione)-zinc(II) diperchlorate, [Zn(C12H6N2O2)3][ClO4]2
• Authors of publication: Zhen-Shan Peng; Jian-Xiang Liu; Wen-Jun Jiang; Qian Deng; Tie-Jun Cai; Ming-Zhong Huang
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2008
• Journal volume: 223
• Journal issue: 3
• Pages of publication: 228
• a: 10.4974 ± 0.0009 Å
• b: 18.0482 ± 0.0015 Å
• c: 18.8074 ± 0.0016 Å
• α: 90°
• β: 94.547 ± 0.001°
• γ: 90°
• Cell volume: 3552 ± 0.5 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1032
• Residual factor for significantly intense reflections: 0.0522
• Weighted residual factors for significantly intense reflections: 0.1313
• Weighted residual factors for all reflections included in the refinement: 0.1579
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No