Information card for entry 8102343

Structure parameters

• Formula: C129 H114 Au F6 O12 P7 Pd9
• Calculated formula: C129 H114 Au F6.02 O12 P7 Pd9
• Title of publication: Crystal structure of nonacarbonylhexakis(triphenylphosphane)nonapalladiumgold hexafluoridophosphate, [Pd~9~Au(CO)~9~(PPh~3~)~6~](PF~6~)
• Authors of publication: Willocq, Christopher; Hermans, Sophie; Devillers, Michel; Tinant, Bernard
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2008
• Journal volume: 223
• Journal issue: 4
• Pages of publication: 495 - 497
• a: 22.52 ± 0.004 Å
• b: 22.52 ± 0.004 Å
• c: 39.433 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 17319 ± 5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for significantly intense reflections: 0.1246
• Weighted residual factors for all reflections included in the refinement: 0.1287
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No