Information card for entry 8102412

Structure parameters

• Chemical name: μ-Carbonato-bis[diaqua(N,N,N',N'-tetramethylethylenediamine) nickel(II)] perchlorate
• Formula: C40 H120 Cl4 N12 Ni6 O40
• Calculated formula: C6.5 H20 Cl N2 Ni O7.5
• Title of publication: Crystal structure of μ-carbonato-bis[diaqua(N,N,N',N'- tetramethylethylenediamine)nickel(II)] perchlorate, [Ni(C6H16N2)(H2O)2(CO3)0.5]2(ClO4)2
• Authors of publication: Keiko Miyamoto; Ernst Horn; Yutaka Fukuda
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2009
• Journal volume: 224
• Journal issue: 1
• Pages of publication: 131
• a: 11.684 ± 0.002 Å
• b: 19.076 ± 0.003 Å
• c: 6.2971 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1403.5 ± 0.4 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0511
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.1073
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No