Information card for entry 8102466

Structure parameters

• Chemical name: bi-(2,2-bipyridine)-hexa(N-tosyl-glycinato)- bisamarium (III)- diaqua.2,2-bipyridine [Sm~2~(C~12~H~8~N~2~)~2~(C~9~H~10~NO~4~S)~6~.H~2~O].(C~12~H~8~N~2~)
• Formula: C42 H44 N6 O13 S3 Sm
• Calculated formula: C42 H44 N6 O13 S3 Sm
• Title of publication: Crystal structure of diaqua-bis(2,2'-bipyridine)-hexa(N-tosylglycinato)disamarium(III) — 2,2'-bipyridine (1:1), Sm2(H2O)2(C10H8N2)2(C9H10NO4S)6 · C10H8N2
• Authors of publication: Gui-Lin Wen; Xia Bao
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2009
• Journal volume: 224
• Journal issue: 3
• Pages of publication: 478
• a: 14.147 ± 0.005 Å
• b: 29.232 ± 0.011 Å
• c: 12.716 ± 0.005 Å
• α: 90°
• β: 115.283 ± 0.006°
• γ: 90°
• Cell volume: 4755 ± 3 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1018
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.0921
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No