Information card for entry 8102496

Structure parameters

• Chemical name: (1,8-dimethyl-1,3,6,8,10,13-hexaazacyclotetradecane)nickel(II) diperchlorate
• Formula: C10 H26 Cl2 N6 Ni O8
• Calculated formula: C10 H26 Cl2 N6 Ni O8
• Title of publication: Crystal structure of (1,8-dimethyl-1,3,6,8,10,13-hexaazacyclotetradecane)nickel(II) diperchlorate, [Ni(C10H26N6)][ClO4]2
• Authors of publication: Zhaowei Yan; Taohai Li
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2009
• Journal volume: 224
• Journal issue: 3
• Pages of publication: 505
• a: 8.536 ± 0.005 Å
• b: 8.73 ± 0.005 Å
• c: 12.736 ± 0.007 Å
• α: 90°
• β: 102.45 ± 0.011°
• γ: 90°
• Cell volume: 926.8 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0523
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.1378
• Weighted residual factors for all reflections included in the refinement: 0.1416
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No