Information card for entry 8102535

Structure parameters

• Chemical name: Bis[ [2-(2-Chloro-6-fluorophenyl)-1H-imidazo[4,5-f][1,10]phenanthroline] [2-(2-Chloro-6-fluorophenyl)-imidazo[4,5-f][1,10]phenanthroline] -lead(II)-hemi-adipicato)]] ‒ water (1:3.5)
• Formula: C82 H53 Cl4 F4 N16 O11 Pb2
• Calculated formula: C82 H46 Cl4 F4 N16 O11 Pb2
• Title of publication: Crystal structure of bis[[2-(2-chloro-6-fluorophenyl)-1H-imidazo[4,5-f][1,10]phenanthroline][2-(2-chloro-6-fluorophenyl)-imidazo[4,5-f][1,10]phenanthroline]]-(adipato)dilead(II) heptahydrate, Pb2(C19H10N4FCl)2(C19H9N4FCl)2(C6H8O4) · 7H2O
• Authors of publication: Zhan-Lin Xu; Xiao-Yuan Ma; Xiu-Yan Wang
• Journal of publication: Zeitschrift für Kristallographie - New Crystal Structures
• Year of publication: 2009
• Journal volume: 224
• Journal issue: 4
• Pages of publication: 613
• a: 18.192 ± 0.005 Å
• b: 8.183 ± 0.002 Å
• c: 26.83 ± 0.007 Å
• α: 90°
• β: 100.291 ± 0.004°
• γ: 90°
• Cell volume: 3929.8 ± 1.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0943
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1259
• Weighted residual factors for all reflections included in the refinement: 0.1427
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No